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Chlorotriethylsilane → n,n-Diethyl-2-chloro-6-(triethylsilyl)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chlorotriethylsilane | HCID 13819 | — |
| 反応物 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 生成物 | n,n-Diethyl-2-chloro-6-(triethylsilyl)benzamide | HCID 18630182 | — |
反応手順
The title compound was prepared according to General Method A from the compound of Example e and 1.4 eq chlorotriethylsilane. Purification by HPLC with 1:19 ethyl acetate/hexanes gave 6.0 g of the desired product as a clear oil, a 92% yield.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06410558B1 |
| 出典データセット | uspto-grants-2002_06 |
| ORD ID | ord-cf1240fa6867476aad97b96d49ae4e1c |
| 出典メモ | uspto-grants-2002_06 |