HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54418911, compound → gamma-(1-Naphthyl)butyric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54418911 | HCID 54418911 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | gamma-(1-Naphthyl)butyric acid | HCID 13077 | 89.8% |
Reaction Steps
To a solution of 4-(1-naphthyl)butenoic acid (3.96 g) in ethyl alcohol (45 cm3) was added palladium on carbon (10%, 400 mg). The mixture was stirred under hydrogen (approx. 2 atm) for 3 h. The catalyst was then removed by filtration through a pad of Dicalite® and the solvent was removed under reduced pressure to yield the title compound (3.59 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06410592B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-687293b14657471c9b0be82c989f2faa |
| Source note | uspto-grants-2002_06 |