HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)phenylhydrazine → 4-(Trifluoromethyl)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)phenylhydrazine | HCID 136200 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(Trifluoromethyl)aniline | HCID 9964 | 100% |
Reaction Steps
Raney nickel (2 g) was added to a solution of 4-trifluoromethylphenylhydrazine (1 g) in methanol (5 ml) and heated at reflux for 1 hour. The cooled mixture was filtered and evaporated to give the title compound in 100% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06410737B1 |
| Source dataset | uspto-grants-2002_06 |
| ORD ID | ord-6b0bc3e7a6ff4574a7acf176eabbca6b |
| Source note | uspto-grants-2002_06 |