HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butoxycarbonyl-L-isoleucine → HCID 178446792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butoxycarbonyl-L-isoleucine | HCID 2724762 | — |
| Reactant | HCID 178469704 | HCID 178469704 | — |
| Product | HCID 178446792 | HCID 178446792 | 40% |
Reaction Steps
The product of Example 5, step b) was treated by the same method as that described in Example 5, step c) except N-Boc-L-Isoleucine (3.70 g, 16 mmol) was used to give the sub-title compound as a light yellow solid (0.29 g, 40%). The product obtained after chromatography still contained impurities and was used for the next step without further purification. MS: ESI (positive): 610 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324210B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-440b49a16a6a46c1b15597181e74cb12 |
| Source note | uspto-grants-2012_12 |