HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) ester, (2S)- → Pyrrolidine-1,2-dicarboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Pyrrolidinedicarboxylic acid, 1-(1,1-dimethylethyl) ester, (2S)- | HCID 85083 | — |
| Reactant | HCID 178469704 | HCID 178469704 | — |
| Product | Pyrrolidine-1,2-dicarboxylic acid | HCID 14794868 | 321.1% |
Reaction Steps
The product of Example 5, step b) was treated by the same method as that described in Example 10, step a) except N-Boc-L-Proline (12.6 g, 5.87 mmol) was used to give the sub-title compound as a pale yellow solid (3.0 g, 60%). MS: ESI (positive): 791 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324210B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-c8ba5ea9e3204ee78dc2a52a6b18696e |
| Source note | uspto-grants-2012_12 |