HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-benzylaminosulfonamide → Benzylsulfamide potassium salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-benzylaminosulfonamide | HCID 12354987 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Product | Benzylsulfamide potassium salt | HCID 21041359 | 100.6% |
Reaction Steps
To a solution of benzylsulfamide (17.98 g) in McOH (300 mL) was carefully added potassium tert-butylate (10.8 g). The mixture was stirred at rt for 15 min before the solvent was evaporated. The remaining residue was dried under HV to give benzylsulfamide potassium salt as an off-white powder (21.73 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324232B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-5d1afc6e2d174f638edd86682471e518 |
| Source note | uspto-grants-2012_12 |