Urea → HCID 178488028, compound

Participants

Reaction Steps

2-Amino-5-methoxybenzoic acid (5.090 g, 30.45 mmol) was heated with urea (18.300 g, 304.50 mmol) to 150° C. for 24 h. Water (150 mL) was cautiously added to the melt and allowed to cool. The resulting precipitate was filtered off and dried to give a solid (4.189 g, 72%).

Provenance & Evidence