HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131730087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21061057 | HCID 21061057 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131730087 | HCID 131730087 | — |
Reaction Steps
A mixture of 0.5 g (1.6 mmol) 1-tert-butyl 4-ethyl 4-(cyclopropylmethyl)piperidine-1,4-dicarboxylate (commercially available) in 20 mL dioxane was treated with 4 mL 4N HCl in dioxane and stirred at room temperature over night. The mixture was evaporated to dryness and used without further purification in the consecutive step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324250B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-ee80fb416204499da46591ef2c6d41d2 |
| Source note | uspto-grants-2012_12 |