HRID2189982

反应详情

EQUATION

反应方程式

HRID 2189982 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 0.5 g (1.6 mmol) 1-tert-butyl 4-ethyl 4-(cyclopropylmethyl)piperidine-1,4-dicarboxylate (commercially available) in 20 mL dioxane was treated with 4 mL 4N HCl in dioxane and stirred at room temperature over night. The mixture was evaporated to dryness and used without further purification in the consecutive step.

WORKUP

后处理

  1. customThe mixture was evaporated to dryness
  2. customused without further purification in the consecutive step