HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57387821, compound → HCID 57388052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57387821 | HCID 57387821 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57388052 | HCID 57388052 | 88% |
Reaction Steps
Using tert-butyl [3-({2-[(cyclopropylcarbonyl)amino]-1-methyl-1H-benzimidazol-6-yl}oxy)phenyl]carbamate (1.52 g, 3.60 mmol) and trifluoroacetic acid (50 mL) as starting materials, and in the same manner as in Example C1(vi), the title compound (1.02 g, 88%) was obtained as a pink amorphous substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324395B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-35fd208fc7d04512a17cb1e070e13839 |
| Source note | uspto-grants-2012_12 |