HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 5213538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Reactant | 6-chloro-N-(4-iodo-3-methyl-phenyl)-nicotinamide | HCID 59318138 | — |
| Product | HCID 5213538 | HCID 5213538 | — |
Reaction Steps
6-Chloro-N-phenyl-nicotinamide was prepared from aniline and 6-chloronicotinoyl chloride following a procedure similar to the one described in the synthesis of 6-chloro-N-(4-iodo-3-methyl-phenyl)-nicotinamide, above. The product was isolated after precipitation out of small volume of CH2Cl2 with hexanes. HRMS m/z calcd for C12H9N2OCl [M+H]+: 233.0476. Found: 233.0476
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324385B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-c4516ecf6f7e499c8c42169157b9c56a |
| Source note | uspto-grants-2012_12 |