HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-4-iodoaniline → HCID 59318151, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-4-iodoaniline | HCID 185694 | — |
| Reactant | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
| Reactant | 6-chloro-N-(4-iodo-3-methyl-phenyl)-nicotinamide | HCID 59318138 | — |
| Product | HCID 59318151 | HCID 59318151 | — |
Reaction Steps
6-Chloro-N-(2-fluoro-4-iodo-phenyl)-nicotinamide was prepared from 2-fluoro-4-iodo aniline and 6-chloronicotinoyl chloride following a procedure similar to the one described in the synthesis of 6-chloro-N-(4-iodo-3-methyl-phenyl)-nicotinamide, above. The product was isolated after precipitation out of a small volume of CH2Cl2 with hexanes. HRMS m/z calcd for C12H7N2OFClI [M+H]+: 376.9349. Found: 376.9349.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324385B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-32ff8a3418b04fba9f27113181b3ec09 |
| Source note | uspto-grants-2012_12 |