HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dimethylfuran → 2,5-Furandimethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dimethylfuran | HCID 12266 | — |
| Reactant | 5-(Hydroxymethyl)furfural | HCID 237332 | — |
| Product | 2,5-Furandimethanol | HCID 74663 | — |
Reaction Steps
In another aspect, the present disclosure provides a method C for preparing 2,5-dimethylfuran, which includes the steps of: a) combining 5-(hydroxymethyl)furfural (HMF) with H2, a first catalyst, and an aprotic solvent; b) reacting the mixture of step (a) to form 2,5-bis(hydroxymethyl)furan (BHMF); c) adding a carboxylic acid, and a second catalyst to the reaction mixture of step (b) to form an ester of BHMF; and d) adding H2 to the reaction mixture that includes the ester of BHMF of step (c) to form 2,5-dimethylfuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08324409B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-7b6d076b65a64f339fe534a6c8d1f7c2 |
| Source note | uspto-grants-2012_12 |