HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → Benzyl 6-hydroxyhexanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | epsilon-CAPROLACTONE | HCID 10401 | — |
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Product | Benzyl 6-hydroxyhexanoate | HCID 15224618 | — |
Reaction Conditions
| Temperature | 100 °C |
|---|
Reaction Steps
A mixture of ε-caprolactone (a) (40 g), benzyl alcohol and p-toluenesulfonic acid monohydrate (0.7 g) was stirred at 100° C. for 16 hours. The reaction mixture was treated in the conventional manner and was distilled under reduced pressure (1 mmHg, 140°-154° C.) to give the title compound (b).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05426115 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-f736997e3a4b4b3e92436d39f969c91d |
| Source note | uspto-grants-1995_06 |