反应详情

温度

100 °C

A mixture of ε-caprolactone (a) (40 g), benzyl alcohol and p-toluenesulfonic acid monohydrate (0.7 g) was stirred at 100° C. for 16 hours. The reaction mixture was treated in the conventional manner and was distilled under reduced pressure (1 mmHg, 140°-154° C.) to give the title compound (b).

1. additionThe reaction mixture was treated in the conventional manner
2. distillationwas distilled under reduced pressure (1 mmHg, 140°-154° C.)