HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1350473-55-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 67002375 | HCID 67002375 | — |
| Product | 1350473-55-0 | HCID 67002050 | 98% |
Reaction Steps
In a 10 mL round-bottomed flask (1-cyclopropanecarbonyl-cyclopentyl)-carbamic acid tert-butyl ester (61 mg, 0.24 mmol) was dissolved in 1.0 M HCl solution in MeOH (1.5 mL, 1.5 mmol). The reaction mixture was stirred at room temperature overnight then concentrated under reduced pressure to afford 45 mg (98%) of (1-amino-cyclopentyl)-cyclopropyl-methanone hydrochloride as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329699B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-9812656e644648a8b9d6765215e936ea |
| Source note | uspto-grants-2012_12 |