HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68956418, compound → HCID 68959277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68956418 | HCID 68956418 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68959277 | HCID 68959277 | — |
Reaction Steps
Trifluoroacetic acid 10 mL was added to the obtained tert-butyl 4-(3-cyanophenyl)-2-(4-fluoroanilino)benzoate, and it was stirred at room temperature for 1 hour. The solvent was removed under reduced pressure, methanol was added to the obtained residue, and solid matter was filtrated to give 4-(3-cyanophenyl)-2-(4-fluoroanilino)benzoic acid 13 mg of pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-fe2bb9064cf4492b9d74e47692d0721c |
| Source note | uspto-grants-2012_12 |