HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68960562, compound → HCID 57668005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68960562 | HCID 68960562 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57668005 | HCID 57668005 | 96.9% |
Reaction Steps
Trifluoroacetic acid 10 mL was added to tert-butyl 4-(2-cyclopenten-1-yl)-2-(4-fluoroanilino)benzoate 27 mg, and it was stirred at room temperature for 1 hour. The solvent was removed under reduced pressure, methanol was added to the obtained residue, and solid matter was filtrated to give 4-(2-cyclopenten-1-yl)-2-(4-fluoroanilino)benzoic acid 22 mg of white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-2329f8b79f1b49b38d6720f3fab58c29 |
| Source note | uspto-grants-2012_12 |