HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57667999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Tert-butyl 2-(benzylamino)-4-phenethylbenzoate | HCID 68961718 | — |
| Product | HCID 57667999 | HCID 57667999 | 80.4% |
Reaction Steps
Trifluoroacetic acid 2.0 mL was added to tert-butyl 2-(benzylamino)-4-phenethylbenzoate 0.16 g, it was stirred at room temperature 4 hours, and the solvent was removed under reduced pressure. Toluene was added to it, and the solvent was removed under reduced pressure. Diisopropyl ether and hexane were added to the obtained residue, solid matter was filtrated to give 2-(benzylamino)-4-phenethylbenzoic acid 0.11 g of white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-edfd729b472742c287c9044e934bd238 |
| Source note | uspto-grants-2012_12 |