HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68958210, compound → HCID 68963099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68958210 | HCID 68958210 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 68963099 | HCID 68963099 | — |
Reaction Steps
Trifluoroacetic acid 10 mL was added to the obtained tert-butyl 2-(2,4-difluoroanilino)-4-phenethylbenzoate, and it was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure, methanol was added to the obtained residue, and solid matter was filtrated to give 2-(2,4-difluoroanilino)-4-phenethylbenzoic acid 59 mg of white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-9ab25a44f7c44f87bd25d9a2c307cfd3 |
| Source note | uspto-grants-2012_12 |