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HRID2191726

反应详情

EQUATION

反应方程式

HRID 2191726 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)c1ccc(/C=C/c2ccc3c(c2)OCCO3)cc1Nc1ccc(F)cc1
HCID68963963

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)c1ccc(/C=C/c2ccc3c(c2)OCCO3)cc1Nc1ccc(F)cc1
HCID57668106

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=C(O)C(F)(F)F
溶剂HCID6422

未命名化合物

PROCEDURE

实验过程

Trifluoroacetic acid 10 mL solution of the obtained tert-butyl 4-((E)-2-(2,3-dihydrobenzo[1,4]dioxin-6-yl)vinyl)-2-(4-fluoroanilino)benzoate was stirred at room temperature for 1 hour. The solvent was removed under reduced pressure to give 4-((E)-2-(2,3-dihydrobenzo[1,4]dioxin-6-yl)vinyl)-2-(4-fluoroanilino)benzoic acid 17 mg of pale yellow solid.

WORKUP

后处理

  1. customThe solvent was removed under reduced pressure