HRID2191746

反应详情

EQUATION

反应方程式

HRID 2191746 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Trifluoroacetic acid 10 mL was added to the obtained tert-butyl 2-(4-methylanilino)-4-phenylbenzoate, and it was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure,diisopropyl ether was added to the obtained residue, and solid matter was filtrated to give 2-(4-methylanilino)-4-phenylbenzoic acid 8.7 mg of white solid.

WORKUP

后处理

  1. customThe solvent was removed under reduced pressure,diisopropyl ether
  2. additionwas added to the obtained residue, and solid matter
  3. filtrationwas filtrated