HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68961390, compound → HCID 57667820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68961390 | HCID 68961390 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57667820 | HCID 57667820 | — |
Reaction Steps
Trifluoroacetic acid 10 mL was added to the obtained tert-butyl 2-(4-fluoroanilino)-4-(3-fluorophenyl)benzoate, and it was stirred at room temperature for 2 hours. The solvent was removed under reduced pressure, hexane was added to the obtained residue, and solid matter was filtrated to give 2-(4-fluoroanilino)-4-(3-fluorophenyl)benzoic acid 56 mg of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-84918954e9ad422d862cf3ef0e3eb2d0 |
| Source note | uspto-grants-2012_12 |