HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57668033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68958028 | HCID 68958028 | — |
| Product | HCID 57668033 | HCID 57668033 | — |
Reaction Steps
Trifluoroacetic acid 5.0 mL was added to the obtained tert-butyl 4-(4-(methanesulfonamido)phenyl)-2-(2-methylanilino)benzoate, and it was stirred at room temperature for 3 hours. The solvent was removed under reduced pressure,diisopropyl ether was added to the obtained residue, solid matter was filtrated to give 4-(4-(methanesulfonamido)phenyl)-2-(2-methylanilino)benzoic acid 52 mg of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-cb285130230e4a5c8e0dd008547bf701 |
| Source note | uspto-grants-2012_12 |