HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57668061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 68962151 | HCID 68962151 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57668061 | HCID 57668061 | 61.7% |
Reaction Steps
Trifluoroacetic acid 2.0 mL was added to dichloromethane 2.0 mL solution of tert-butyl 2-((biphenyl-4-yl)amino)-4-phenethylbenzoate 50 mg, and it was stirred at room temperature for 4 hours and 30 minutes. The solvent was removed under reduced pressure,diisopropyl ether was added to the obtained residue, and solid matter was filtrated to give 2-((biphenyl-4-yl)amino)-4-phenethylbenzoic acid 27 mg of a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08327467B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-feb208daae10435883fa1018dfd8040f |
| Source note | uspto-grants-2012_12 |