HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Nitrobenzimidazole → HCID 178507353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Nitrobenzimidazole | HCID 7195 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178507353 | HCID 178507353 | 100% |
Reaction Steps
A solution of 5-nitrobenzimidazole (10.0 g, 613 mmol) in methanol (250 mL) was hydrogenated in the presence of 10% Pd/C (0.40 g) at atmospheric pressure for 20 h. The mixture was filtered through Celite® and the solvent removed under reduced pressure to afford the pure product (8.1 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329737B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-e0d76ab6f3bf4b7e8fa053a7f21fe6e1 |
| Source note | uspto-grants-2012_12 |