Hydrogen chloride-ethyl acetate → HCID 68432360, compound

Participants

Reaction Steps

tert-Butyl 3-ethyl-4-({4-[(2-furylmethyl)amino]-2-isopropylpyrimidin-5-yl}carbonyl)piperazine-1-carboxylate (100 mg) was dissolved in 4 M hydrogen chloride-ethyl acetate solution (3 ml), and the mixture was stirred at room temperature for 15 hr. The reaction mixture was concentrated under reduced pressure, ethyl acetate was added and the precipitate was collected by filtration to give the object compound (74 mg).

Provenance & Evidence