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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2192851Generated: November 4, 2026

Hydrochloride methanol → HCID 68432464, compound

https://huagongshe.com/reaction/2192851

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloride methanolHCID 21893726—
ReactantHCID 59625477HCID 59625477—
ProductHCID 68432464HCID 68432464—

Reaction Steps

tert-Butyl (3S,5R)-3-[({2-tert-butyl-4-[(3-methoxypropyl)amino]pyrimidin-5-yl}carbonyl)(2-methylpropyl)amino]-5-[(4-hydroxy-4-methylpiperidin-1-yl)carbonyl]piperidine-1-carboxylate (113 mg) was dissolved in 10% hydrogen chloride-methanol solution (4.5 ml), and the mixture was stirred at room temperature for 18 hr. The solvent was evaporated under reduced pressure, and the residue was dried under reduced pressure to give the object compound (82 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08329691B2
Source datasetuspto-grants-2012_12
ORD IDord-08642e5f043640aa8a96b9acaea482ab
Source noteuspto-grants-2012_12