HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloride methanol → HCID 68432464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloride methanol | HCID 21893726 | — |
| Reactant | HCID 59625477 | HCID 59625477 | — |
| Product | HCID 68432464 | HCID 68432464 | — |
Reaction Steps
tert-Butyl (3S,5R)-3-[({2-tert-butyl-4-[(3-methoxypropyl)amino]pyrimidin-5-yl}carbonyl)(2-methylpropyl)amino]-5-[(4-hydroxy-4-methylpiperidin-1-yl)carbonyl]piperidine-1-carboxylate (113 mg) was dissolved in 10% hydrogen chloride-methanol solution (4.5 ml), and the mixture was stirred at room temperature for 18 hr. The solvent was evaporated under reduced pressure, and the residue was dried under reduced pressure to give the object compound (82 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329691B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-08642e5f043640aa8a96b9acaea482ab |
| Source note | uspto-grants-2012_12 |