HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenyl Isocyanate → HCID 66661923, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenyl Isocyanate | HCID 7693 | — |
| Reactant | HCID 58056911 | HCID 58056911 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 66661923 | HCID 66661923 | 46% |
Reaction Steps
Starting material 8 (1 g, 3.6 mmol) was dissolved in 12 ml of pyridine and p-chlorphenyl isocyanate (546 mg, 3.6 mmol) was added. The red solution was stirred over the weekend. The solvent was reduced in a vacuum centrifuge. The crude product was used without further purification (green-brown solid, 1.13 g, 65% content 9, 46% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329907B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-3515c5d8e048488d9b68b8d461c35f84 |
| Source note | uspto-grants-2012_12 |