HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzenesulfonyl chloride → HCID 59577989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzenesulfonyl chloride | HCID 76187 | — |
| Reactant | HCID 53393794 | HCID 53393794 | — |
| Reactant | 4-(2-Methoxy-ethyl)-piperidine-4-carboxylic acid ethyl ester | HCID 56753969 | — |
| Product | HCID 59577989 | HCID 59577989 | — |
Reaction Steps
Light brown crystalline solid. MS (ESI): 473.2 (MH+). This example was prepared in analogy to example 1 step C) to D) from 4-(2-methoxy-ethyl)-piperidine-4-carboxylic acid ethyl ester (example 1 step B)), 2-chlorobenzenesulfonyl chloride and 1-ethyl-1H-indazol-5-ylamine (for synthesis: Chakrabarty et al. Tetrahedron; 64; 2008; 6711).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08329904B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-da76ef01e15c49bba3ed5ff97951d4ea |
| Source note | uspto-grants-2012_12 |