HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-3-fluorobenzene → 4-[4-(3-fluoro-phenylethynyl)-2,5-dimethyl-imidazol-1-yl]-1-methyl-1H-pyridin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-3-fluorobenzene | HCID 520218 | — |
| Reactant | 4-(4-iodo-2,5-dimethyl-imidazol-1-yl)-1-methyl-1H-pyridin-2-one | HCID 66865995 | — |
| Product | 4-[4-(3-fluoro-phenylethynyl)-2,5-dimethyl-imidazol-1-yl]-1-methyl-1H-pyridin-2-one | HCID 49872671 | — |
Reaction Steps
The title compound, brown waxy solid, MS: m/e=322.1 (M+H+), was prepared in accordance with the general method of example 1c from 4-(4-iodo-2,5-dimethyl-imidazol-1-yl)-1-methyl-1H-pyridin-2-one and 1-Ethynyl-3-fluoro-benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334287B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-2d45fe685a7c4f0b8f865e2983a19c4e |
| Source note | uspto-grants-2012_12 |