HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2194521Generated: October 29, 2026
HCID 67009976, compound → HCID 86659346, compound
https://huagongshe.com/reaction/2194521
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 67009976 | HCID 67009976 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86659346 | HCID 86659346 | 93% |
Reaction Steps
8.03 g (32.9 mmol) of (2-(2-methoxybenzylamino)-3-pyridinyl)methanol was dissolved in chloroform (100 mL), and 8.60 g (98.7 mmol) of manganese dioxide was added thereto. The resulting mixture was stirred overnight at 60° C. The reaction mixture was filtered, and the filtrate was concentrated. Thus, 7.40 g (yield: 93%) of the title compound was obtained as an orange-colored solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08334236B2 |
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| Source dataset | uspto-grants-2012_12 |
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| ORD ID | ord-cc1c68a2c1cb4108a8eb1b57a8e0d7fc |
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| Source note | uspto-grants-2012_12 |
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