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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2194521Generated: October 29, 2026

HCID 67009976, compound → HCID 86659346, compound

https://huagongshe.com/reaction/2194521

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67009976HCID 67009976—
CatalystHCID 178418406HCID 178418406—
SolventChloroformHCID 6212—
ProductHCID 86659346HCID 8665934693%

Reaction Conditions

Temperature60 °C

Reaction Steps

8.03 g (32.9 mmol) of (2-(2-methoxybenzylamino)-3-pyridinyl)methanol was dissolved in chloroform (100 mL), and 8.60 g (98.7 mmol) of manganese dioxide was added thereto. The resulting mixture was stirred overnight at 60° C. The reaction mixture was filtered, and the filtrate was concentrated. Thus, 7.40 g (yield: 93%) of the title compound was obtained as an orange-colored solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08334236B2
Source datasetuspto-grants-2012_12
ORD IDord-cc1c68a2c1cb4108a8eb1b57a8e0d7fc
Source noteuspto-grants-2012_12