HCID 67010052, compound → HCID 87235637, compound

Participants

Reaction Conditions

Reaction Steps

3.3 g (16 mmol) of (2-(5-methyl-3-isoxazolyl)amino-3-pyridinyl)methanol was dissolved in chloroform (60 mL), and 4.3 g (49 mmol) of manganese dioxide was added thereto. The resulting mixture was stirred for 48 hours at 60° C. The reaction mixture was filtered, and the filtrate was concentrated. Thus, 3.3 g of the title compound was obtained as an orange-colored viscous product (yield: quantitative).

Provenance & Evidence