HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2194627Generated: November 2, 2026
Cyclohexanecarboxylic acid → Cyclohexanecarbonyl chloride
https://huagongshe.com/reaction/2194627
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cyclohexanecarboxylic acid | HCID 7413 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | Cyclohexanecarbonyl chloride | HCID 75938 | — |
Reaction Steps
The mixture of cyclohexylcarboxylic acid (40 g) and SOCl2 (60 mL) was heated at 30° C. for 30 min and then at 50° C. for 3-5 hrs. The volatile materials were removed in vacuum and the residue was used for the next reaction without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08334307B2 |
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| Source dataset | uspto-grants-2012_12 |
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| ORD ID | ord-2dfdb0f3bd504bb690ccf095415b8a56 |
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| Source note | uspto-grants-2012_12 |
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