HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86631605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86631600 | HCID 86631600 | — |
| Reactant | HCID 178527881 | HCID 178527881 | — |
| Product | HCID 86631605 | HCID 86631605 | 100.1% |
Reaction Steps
With 5-bromo-4-(2-fluoropyridin-3-yl)thiophene-2-carbaldehyde (250 mg) as a starting material, and using 2-mercaptothiazole (134 mg) and potassium carbonate (193 mg), an operation similar to that of Reference Example 1 was performed to give the title compound as a white powder (yield 282 mg, yield 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334301B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-d5e5914ad6684a4cab11bfbaa55c5a7a |
| Source note | uspto-grants-2012_12 |