HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 86644412, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86631600 | HCID 86631600 | — |
| Product | HCID 86644412 | HCID 86644412 | 99% |
Reaction Steps
With 5-bromo-4-(2-fluoropyridin-3-yl)thiophene-2-carbaldehyde (2.86 g) as a starting material, and using thiophenol (1.33 mL) and potassium carbonate (2.21 g), an operation similar to that of Reference Example 1 was performed to give the title compound as a pale-yellow oil (yield 3.11 g, yield 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334301B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-accf0c1595f143e48979bbbceb051ef6 |
| Source note | uspto-grants-2012_12 |