HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-Indazole → HCID 25215201, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-Indazole | HCID 9221 | — |
| Reactant | HCID 67050527 | HCID 67050527 | — |
| Product | HCID 25215201 | HCID 25215201 | — |
Reaction Steps
This compound was made by a procedure similar to that used to prepare 6-chloro-1-(3-ethyl-5-isopropyl-2,6-dioxo-1,2,3,6-tetrahydro-pyrimidin-4-yl)-1H-indole-4-carbonitrile (90), except that 1H-indazole was used instead of 6-chloro-1H-indole-4-carbonitrile. LC-MS shows 299.1 (M+1). 1H NMR (300 MHz, CDCl3): δ 8.97 (br, 1H), 8.31 (s, 1H), 7.83 (d, 2H), 7.54 (m, 1H), 7.36 (m, 2H), 3.42 (m, 1H), 3.20 (m, 1H), 1.90 (m, 1H), 1.15 (dd, 6H), 1.00 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334295B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-1bebc98f5c664aeaa736aac4c08ae9cf |
| Source note | uspto-grants-2012_12 |