HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole → HCID 58203437, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole | HCID 798 | — |
| Reactant | HCID 67050527 | HCID 67050527 | — |
| Product | HCID 58203437 | HCID 58203437 | — |
Reaction Steps
This compound was made by a procedure similar to that used to prepare 6-chloro-1-(3-ethyl-5-isopropyl-2,6-dioxo-1,2,3,6-tetrahydro-pyrimidin-4-yl)-1H-indole-4-carbonitrile (90), except that 1H-indole was used instead of 6-chloro-1H-indole-4-carbonitrile. LC-MS shows 298.2 (M+1). 1H NMR (300 MHz, CDCl3): δ 8.32 (br, 1H), 7.72 (d, 1H), 7.25 (m, 2H), 7.19 (m, 1H), 6.80 (m, 1H), 3.50 (m, 1H), 3.18 (m, 1H), 1.97 (m, 1H), 1.17 (dd, 6H), 1.03 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08334295B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-868a81d71adc4c40887c8e5be4bc733f |
| Source note | uspto-grants-2012_12 |