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HRID2195686

反应详情

EQUATION

反应方程式

HRID 2195686 的结构方程式

REACTANTS

反应物

2
结构：C1=CCCCC1
HCID8079

Cyclohexene

C6H10

结构：CC1CN(c2ccc([N+](=O)[O-])c(C(=O)O)c2)CC(C)O1
HCID43176711

5-(2,6-Dimethylmorpholin-4-yl)-2-nitrobenzoic acid

C13H16N2O5

PRODUCTS

生成物

1
结构：CC1CN(c2ccc(N)c(C(=O)O)c2)CC(C)O1
HCID54888441

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Pd]
催化剂HCID23938

Palladium

Pd

PROCEDURE

实验过程

The mixture of 6 g 2-nitro-5-(2,6-dimethylmorpholin-4-yl)benzoic acid, 15 ml cyclohexene and 3 g Pd/C (10%) is heated under reflux for 6 hours. The hot reaction mixture is filtered through a celite pad. After evaporation of the filtrate 4.8 g title product is obtained (MH+: 251).

WORKUP

后处理

  1. temperatureis heated
  2. temperatureunder reflux for 6 hours
  3. filtrationThe hot reaction mixture is filtered through a celite pad
  4. customAfter evaporation of the filtrate 4.8 g title product
  5. customis obtained (MH+: 251)