Hydrochloric Acid → HCID 86652069, compound

Participants

Reaction Steps

A solution of 90 mg of [3-[(2-quinolin-3-yl)imidazo[1,2-a]pyridin-6-yl]phenyl]methanol in dichloromethane and methanol is passed through sintered glass and then 5.2 ml of a 0.1N solution of hydrochloric acid in isopropanol is added to the filtrate. A precipitate forms, and is collected by filtration and washed with diethyl ether. The solid is then dissolved at ambient temperature with the minimum amount of methanol and then taken up with diethyl ether. The precipitate is recovered by filtration and oven-dried under reduced pressure. 66 mg of compound are obtained.

Provenance & Evidence