HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 44230599, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 44230600 | HCID 44230600 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 44230599 | HCID 44230599 | — |
Reaction Steps
156 mg of [2-(2-furan-3-ylimidazo[1,2-a]pyridin-6-yl)phenyl]methanol are suspended in dichloromethane; 5.4 ml of a 0.1N solution of hydrochloric acid in isopropanol are added thereto, dropwise, and the mixture is stirred at ambient temperature. The reaction mixture is then concentrated under reduced pressure. The residual solid is taken up in diethyl ether and the precipitate is recovered by filtration, washed with diethyl ether and oven-dried under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338451B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-6724f64f203c45e29d2169668de8875b |
| Source note | uspto-grants-2012_12 |