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HRID2196508

反应详情

EQUATION

反应方程式

HRID 2196508 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc(B(O)O)s1
HCID2773430

5-Formyl-2-thiopheneboronic acid

C5H5BO3S

结构：CC(C)(C)OC(=O)NN(C(=O)OC(C)(C)C)c1csc(C=O)c1
HCID59843289

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NN(C(=O)OC(C)(C)C)c1ccc(C=O)s1
HCID59843212

未命名化合物

收率 47%

PROCEDURE

实验过程

Following the same procedure as described for compound 11 (step 1, scheme 2, example 1c) except using 5-formyl-2-thiopheneboronic acid (1.80 g, 11.5 mmol) instead of 5-formylthiophen-3-ylboronic acid to afford 19 (935 mg, 47%) as an orange solid. LRMS (ESI): calc. 342.1; found 343.2 (MH)+.