HuagongsheHuagongshe Chemistry Print Report · For research reference only
Di-tert-butyl 1-(5-cyanothiophen-2-yl)hydrazine-1,2-dicarboxylate → HCID 69090430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Di-tert-butyl 1-(5-cyanothiophen-2-yl)hydrazine-1,2-dicarboxylate | HCID 59843233 | — |
| Reactant | HCID 69299496 | HCID 69299496 | — |
| Product | HCID 69090430 | HCID 69090430 | 78% |
Reaction Steps
Following the same procedure as described for compound 13 (step 3, scheme 2, example 1c) except using 20 (692 mg, 2.04 mmol) instead of 12 to afford 21 (278 mg, 78%) as a brown solid. LRMS (ESI): calc. 139.0; found 140.1 (MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338437B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-38a1cb427a69415090af08e47c5bfba8 |
| Source note | uspto-grants-2012_12 |