Trifluoroacetic acid → HCID 59843310, compound

Participants

Reaction Conditions

Reaction Steps

To a stirred solution of 93 (1.014, 2.59 mmol) in CH2Cl2 (13 ml) was added TFA (3 ml, 38.9 mmol). The resulting solution was allowed to stir at 21° C. for 2 h. After the usual work-up, crude 94 was obtained as colorless oil. LRMS (ESI): calc. 291.3; found 292.2 (MH)+.

Provenance & Evidence