Sodium Hydroxide → HCID 59843235, compound

Participants

Reaction Steps

To a stirred suspension of 93 (500 mg, 1.278 mmol) in ethanol (4.3 mL) was added a solution of NaOH (1.916 mL, 2N, 3.83 mmol) and the mixture was stirred at room temperature for 1 h, then it was concentrated and 1N HCl was added till the solution reached PH-1. Extraction with EtOAc and normal work-up gave crude 101 as colorless oil. LRMS (ESI): calc. 363.3; found 386.2 (MNa)+.

Provenance & Evidence