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HRID2196853

反应详情

EQUATION

反应方程式

HRID 2196853 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CC1C(=NOCc2ccccc2)CCN1C(=O)[C@@H](NC(=O)OC(C)(C)C)C1CCCCC1
HCID86623471

未命名化合物

PRODUCTS

生成物

1
结构：N[C@H](C(=O)N1CCCC1C=NOCc1ccccc1)C1CCCCC1
HCID86623470

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

The solution of {(S)-2-[benzyloxylimino-methyl-pyrrolidine-1-yl]-1-cyclohexyl-2-oxo-ethyl}-carbamic acid tert-butyl ester (1.76 g, 3.97 mmole) and TFA (10 ml) in dichloromethane (20 ml) is stirred for a hour. Solvent is removed under vacuum. The residue is carried to next step without further purification. M+H+=344.2

WORKUP

后处理

  1. customSolvent is removed under vacuum
  2. customThe residue is carried to next step without further purification