Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Methyl 2,2,3-trifluoro-3-[1,1,2,2,3,3-hexafluoro-3-(trifluoromethoxy)propoxy]propanoate | HCID 131727912 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178526054 | HCID 178526054 | — |
Reaction Steps
CF3O(CF2)3OCHFCF2COOCH3 (19.6 grams, 50.0 mmol), 15 grams of ethanol, 2.8 grams (50 mmol) of potassium hydroxide, and 2 grams of water were added to a 100-mL, 3-necked flask, equipped with a stirrer, a condenser, and a thermometer. The reaction mixture was heated on a heating mantle and stirred for 6 hours at 40° C. A clear, colorless solution of CF3O(CF2)3OCHFCF2COOK was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08338517B2 |
|---|
| Source dataset | uspto-grants-2012_12 |
|---|
| ORD ID | ord-cb6670db64704119867dca3447ffe5a1 |
|---|
| Source note | uspto-grants-2012_12 |
|---|
