HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 24759576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Bromoacetic Acid | HCID 6227 | — |
| Reactant | 4-Methylthiazole | HCID 12748 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 24759576 | HCID 24759576 | 72.3% |
Reaction Steps
15.6 g of 4-methylthiazole was dissolved in 50 ml of anhydrous acetone. The mixture was added with 21 g of bromoacetic acid, stirred for 3 d, filtered to obtain a solid, and a white solid was then obtained by recrystallization from ethanol, and dried to obtain 26 g product with a yield of 72%, mP=240.6-241.6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338616B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-ac76e6e779c44084a5cb9fa735c382cf |
| Source note | uspto-grants-2012_12 |