Ammonium Chloride → HCID 68460649, compound

HRID 2197749Notes

Reaction equation

HRID 2197749 reaction equation

[F:1][C:2]1[CH:3]=[C:4]([NH:20][C:21](=[O:23])[CH3:22])[CH:5]=[C:6]([F:19])[C:7]=1[S:8][C:9]1[CH:14]=[CH:13][C:12]([CH3:15])=[CH:11][C:10]=1[N+:16]([O-])=O.[NH4+].[Cl-]>[Fe]>[NH2:16][C:10]1[CH:11]=[C:12]([CH3:15])[CH:13]=[CH:14][C:9]=1[S:8][C:7]1[C:2]([F:1])=[CH:3][C:4]([NH:20][C:21](=[O:23])[CH3:22])=[CH:5][C:6]=1[F:19]

Participants

4

Reactant 2

HCID 25517Ammonium Chloride

HCID 68455821HCID 68455821, compound

Product 1

HCID 68460649HCID 68460649, compound

Reagents, catalysts & solvents 1

HCID 23925IronCatalyst

Procedure

The product from Example 40a was reduced with Fe and NH4Cl following the procedure from Example 237E to give the title compound.

Sources & evidence

ORD record: ord-4217f7188a0445cf81e58566a867036f
Source dataset: uspto-grants-2012_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08338605B2

Reaction notes

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