HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenethiol → 1-(4-Methoxy-phenylsulfanyl)-4-methyl-2-nitro-benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenethiol | HCID 12765 | — |
| Reactant | 4-Methyl-2-nitrophenyl trifluoromethanesulfonate | HCID 71346889 | — |
| Product | 1-(4-Methoxy-phenylsulfanyl)-4-methyl-2-nitro-benzene | HCID 60204792 | 78% |
Reaction Steps
The product from Example 4a (5.0 g, 175 mmol) was reacted with 4-methoxy-benzenethiol (2.45 g, 175 mmol) for 18 h following the procedure from Example 4b giving the product as a solid (3.76 g, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08338605B2 |
| Source dataset | uspto-grants-2012_12 |
| ORD ID | ord-69e1bc86581e4080b5c694a29d900a01 |
| Source note | uspto-grants-2012_12 |